Data File D:\\AGLIENT 1260\\DATA\\20150319\\20150319 2015-03-19 09-00-09\\CPK2015-319-05047.DSample Name: CPK2015-319-05047=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 40Acq. Instrument : HY-LCMS-02 Location : Vial 29Injection Date : 3/19/2015 12:15:07 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150319\\20150319 2015-03-19 09-00-09\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 3/19/2015 9:00:09 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\HY-303_17-H01RS(LCMS).MLast changed : 3/19/2015 1:43:31 PM by Li Shan(LCMS-02) (modified after loading)Method Info : HPLC Catalo No : HY-12034 Batch#05047 A-RP-132 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150319\\20150319 2015-03-19 09-00-09\\CPK2015-319-05047.D) 2.077 1.975 2.204 2.284mAU40030020010000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.975 MM 0.1110 2.57448 3.86394e-1 0.2011 2 2.077 MM 0.0417 12.46033 505.17441 98.7692 3 2.204 MM 0.0479 12.26776 4.26706 0.9583 4 2.284 MM 0.0430 9.14553e-1 3.54419e-1 0.0714 Totals : 1280.21712 510.18228 ===================================================================== *** End of Report ***HY-LCMS-02 3/19/2015 1:43:33 PM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150319\\20150319 2015-03-19 09-00-09\\CPK2015-319-05047.DSample Name: CPK2015-319-05047===========================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 40Acq. Instrument : HY-LCMS-02 Location : Vial 29Injection Date : 3/19/2015 12:15:07 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150319\\20150319 2015-03-19 09-00-09\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 3/19/2015 9:00:09 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\HY-303_17-H01RS(LCMS).MLast changed : 3/19/2015 1:45:26 PM by Li Shan(LCMS-02) (modified after loading)Method Info : HPLC Catalo No : HY-12034 Batch#05047 A-RP-132 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150319\\20150319 2015-03-19 09-00-09\\CPK2015-319-05047.D) ES-API, Pos, Sc 2.0823000002500002000001500001000005000000.511.522.53min HY-LCMS-02 3/19/2015 1:45:28 PM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150319\\20150319 2015-03-19 09-00-09\\CPK2015-319-05047.DSample Name: CPK2015-319-05047MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 2.082 1439827 496.80 I 495.90 I*MSD1 SPC, time=2.054:2.109 of D:\\AGLIENT 1260\\DATA\\20150319\\20150319 2015-03-19 09-00-09\\CPK2015-319-05047.D ES-API100806040200100200300400500600m/z 496.8 495.9Max: 191360 *** End of Report ***HY-LCMS-02 3/19/2015 1:45:28 PM Li Shan(LCMS-02) 497.9Page 2 of 2
